Chemistry Research Laboratory

Homepage: http://www.chem.ox.ac.uk/crl/

Equipment

Agilent 6120

Managed by:

Department of Chemistry, University of Oxford

Availability:

MS services 24 hour turnaround.

Benchtop quadrupole LC-MS, used for small molecule open access.
Agilent 7200 QTOF

Managed by:

Department of Chemistry, University of Oxford

Availability:

Trained user availability variable.

Agilent 7890B Gas chromatograph, Agilent 7200 Accurate Mass QTOF Agilent GC Sampler 120
Agilent Cary 4000

Managed by:

Department of Chemistry, University of Oxford

Availability:

http://saf.chem.ox.ac.uk/booking-oxford.aspx

Cary 4000 UV Vis spectrometer with optional Pike Veemac diffuse IR accessory. Wavelength range 175-900 nm with ± 0.08 nm accuracy. Cell can be used ...
Agilent SuperNova with Oxford Cryosystems Cryostreams

Managed by:

Department of Chemistry, University of Oxford

Availability:

Heavily used during Hilary Term. Generally about 80% usage.

Dual X-ray sources Cu anode and Mo anode (50 W tube, microfocus optics, 50 kV, 1 mA), 2Theta angle: -115° - +157° (0.00125° resolution) Sphere ...
Beaglehole Instruments Picometer Ellipsometer

Managed by:

Department of Chemistry, University of Oxford

Availability:

http://saf.chem.ox.ac.uk/booking-oxford.aspx

Spectroscopic and Single-Wavelength Ellipsometry. Optically flat surfaces are essential. The sensitivity is usually shot noise limited, and typically is equivalent to an ellipticity of about ...
Bio-Rad FTS-6000

Managed by:

Department of Chemistry, University of Oxford

Availability:

http://saf.chem.ox.ac.uk/booking-oxford.aspx

ATR, PMIRRAS and IRAS. For IRAS/PMIRRAS the samples must be optically flat.
Bio-Rad PT7125 Barrel Plasma Etcher

Managed by:

Department of Chemistry, University of Oxford

Availability:

http://saf.chem.ox.ac.uk/booking-oxford.aspx

A 150 W, 13.56 MHz cylindrical plasma chamber designed to produce an isotropic etch.
Bruker AXS D8 ADVANCE

Managed by:

Department of Chemistry, University of Oxford

Availability:

http://saf.chem.ox.ac.uk/booking-oxford.aspx

To determine layer thickness (between 0.5 and 400 nm), density and roughness (between 0 and 2 nm) with about 1% accuracy, independently of each other. ...
Bruker BioSpin AVII500 with cryoprobe

Managed by:

Department of Chemistry, University of Oxford

Availability:

Heavily used.

2-channel instrument equipped with a dedicated 5 mm 13C(1H) dual cryoprobe optimised for 13C detection.
Bruker BioSpin AVIII 500

Managed by:

Department of Chemistry, University of Oxford

Availability:

Heavily used.

2- channel automated spectrometer capable of H/X studies
Bruker BioSpin AVIII 600

Managed by:

Department of Chemistry, University of Oxford

Availability:

Heavily used.
Bruker BioSpin AVIII HD 500

Managed by:

Department of Chemistry, University of Oxford

Availability:

Heavily used.

2- channel instrument equipped with: 5 mm z-gradient BBFO probe
Bruker BioSpin AVIII400

Managed by:

Department of Chemistry, University of Oxford

Availability:

Heavily used.

2-channel 400 MHz automated spectrometer equipped with a multinuclear BBFO probe and 60 position robotic sample changer.
Bruker BioSpin AVIII400

Managed by:

Department of Chemistry, University of Oxford

Availability:

Heavily used.

2-channel 400 MHz automated spectrometer equipped with a multinuclear BBFO probe and 60 position robotic sample changer.
Bruker BioSpin AVIII400

Managed by:

Department of Chemistry, University of Oxford

Availability:

Heavily used.

2-channel 400 MHz automated spectrometer equipped with a multinuclear BBFO probe and 60 position robotic sample changer.
Bruker BioSpin AVIII700 with cryoprobe

Managed by:

Department of Chemistry, University of Oxford

Availability:

Heavily used.

4- channel instrument equipped with a dedicated 5 mm 1H(13C/15N) inverse cryoprobe optimised for 1H observation.
Bruker BioSpin AVIIIHD 500

Managed by:

Department of Chemistry, University of Oxford

Availability:

Heavily used.

3- channel automated spectrometer capable of H/X and H/F/X studies
Bruker BioSpin AVIIIHD Solids HFX 400

Managed by:

Department of Chemistry, University of Oxford

Availability:

Heavily used.

Solid-state 400 Mhz three-channel spectrometer with H/F/X capabilities plus hardware for diffusion and micro- imaging.
Bruker BioSpin AVIIIHD Solids HXY 400

Managed by:

Department of Chemistry, University of Oxford

Availability:

Heavily used.

Solid-state 400 MHz three- channel spectrometer with H/X/Y capabilities
Bruker BioSpin DPX200

Managed by:

Department of Chemistry, University of Oxford

Availability:

Lightly used

2-channel manual instrument equipped with: 5 mm 13C/1H dual probe
Bruker BioSpin NEO400

Managed by:

Department of Chemistry, University of Oxford

Availability:

Heavily used.

2-channel 400 MHz automated spectrometer equipped with a multinuclear BBFO probe and 16 position robotic sample changer.
Bruker Bruker Autoflex

Managed by:

Department of Chemistry, University of Oxford

High resolution tandem time of flight MALDI MS/MS system used primarily for proteomics and peptide analysis.
Bruker Vertex 80

Managed by:

Department of Chemistry, University of Oxford

Availability:

http://saf.chem.ox.ac.uk/booking-oxford.aspx

ATR, PMIRRAS. For IRAS/PMIRRAS the samples must be optically flat. Resolution 0.06cm-1. Full spectral range from UV to far IR
Digital Instruments MultiMode SPM Nanoscope

Managed by:

Department of Chemistry, University of Oxford

Availability:

http://saf.chem.ox.ac.uk/booking-oxford.aspx

Surface Metrology of samples. Allows AFM, STM and magnetic images to be taken. Typically, lateral resolution > 1 nm, height resolution >1 A. Samples must ...
Dionex UltiMate 3000 RSLCnano System

Managed by:

Department of Chemistry, University of Oxford

Availability:

Not available for sharing.

Ultra high pressure nanoflow HPLC providing high performance separations and direct introduction to ESI-MS systems.
Edwards Auto 306

Managed by:

Department of Chemistry, University of Oxford

Availability:

http://saf.chem.ox.ac.uk/booking-oxford.aspx

For evaporation of Chromium and Gold, including substrate cleaning and contaminant-free deposition.
IT Concept TRACKER

Managed by:

Department of Chemistry, University of Oxford

Availability:

http://saf.chem.ox.ac.uk/booking-oxford.aspx

Drop tensiometer. Measurement of low to high interfacial tension (from less than 0.1 mN/m to more than 100 mN/m). <1 ml sample volumes required.
Micromeritics 3flex

Managed by:

Department of Chemistry, University of Oxford

Availability:

http://saf.chem.ox.ac.uk/booking-oxford.aspx

fully automated, three-station instrument capable of high-performance physisorption, mesopore, micropore, and chemisorption analyses. measures specific surface area from 0.01m²/g.
Micromeritics AutoChem 2920

Managed by:

Department of Chemistry, University of Oxford

Availability:

http://saf.chem.ox.ac.uk/booking-oxford.aspx

Fully automated chemisorption analyzer can acquire valuable information about the physical properties of your catalyst, catalyst support, or other materials. Determination of catalytic properties such ...
Micromeritics Tristar

Managed by:

Department of Chemistry, University of Oxford

Availability:

http://saf.chem.ox.ac.uk/booking-oxford.aspx

3 physisorption analysis ports, measures specific surface area from 0.01m²/g.
Nonius Kappa-CCD with Oxford Cryosystems Cryostreams

Managed by:

Department of Chemistry, University of Oxford

Availability:

Heavily used during Hilary Term. Generally about 80% usage.

X-ray source Mo anode (max 60 kV, 300 mA), graphite monochromator, Theta angle: -10° - +66° (± 0.01°) Sphere of Confusion R: 5 µm.
Olympus FluoView FV1200MPE Basic

Managed by:

Department of Chemistry, University of Oxford

Availability:

http://saf.chem.ox.ac.uk/booking-oxford.aspx

Fixed-stage upright multiphoton microscope equipped with a Spectra-Physics MaiTai eHP DeepSee laser (70 fs pulse width, 80 MHz repetition rate, continuously tunable between 690--1040 nm). ...
PANalytical X'Pert PRO

Managed by:

Department of Chemistry, University of Oxford

Availability:

All instruments oversubscribed during period September - June inclusive.

General purpose. Cu alpha 1/2.
Thermo Scientific Delta V Advantage

Managed by:

Department of Chemistry, University of Oxford

Availability:

Not available for sharing.

Isotope ratio mass spectrometer with Surveyor HPLC system and an LC-Isolink interface for compound specific carbon isotope analysis.
Thermo Scientific Exactive

Managed by:

Department of Chemistry, University of Oxford

Availability:

Trained user availability variable.

High sensitivity, very high resolition (140,000) orbitrap detector with HP1100 inlet system.
Thermo Scientific LTQ Orbitrap XL

Managed by:

Department of Chemistry, University of Oxford

Availability:

Not available for sharing.

Hybrid ion trap/orbitrap mass spectrometer for exact/precise mass measurement primarily of peptides to small proteins.
Thermo Scientific Orbitrap Elite

Managed by:

Department of Chemistry, University of Oxford

High sensitivity, very high resloution (250,000). Electron transfer dissociation (ETD). Coupled to Waters NanoAcquity LC.
Thermo Scientific Q-Exactive

Managed by:

Department of Chemistry, University of Oxford

Availability:

Trained user availability variable.

High sensitivity, very high resolition (140,000) orbitrap detector with UPLC (Dionex U3000).
Tuneable Dye Laser System

Managed by:

Department of Chemistry, University of Oxford

Availability:

Configured so can be used on any one of the three experiments in the current laboratory.

With Cobra (Sirah) dye laser and Surelite (Continuum) high energy Nd:YAG laser. Covering wavelength 200-900 nm.
Varian FTS-7000

Managed by:

Department of Chemistry, University of Oxford

Availability:

http://saf.chem.ox.ac.uk/booking-oxford.aspx

ATR, PMIRRAS and IRAS. For IRAS/PMIRRAS the samples must be optically flat.
Waters LCT Premier

Managed by:

Department of Chemistry, University of Oxford

Availability:

Open Access MS

A benchtop instrument with a electrospray source and a TOF analyser. Its used primarily as an LC/MS system for the biological MS service and External ...
Waters LCT Premier

Managed by:

Department of Chemistry, University of Oxford

Availability:

Open Access MS

A benchtop instrument with a electrospray source and a TOF analyser.
Waters LCT Premier

Managed by:

Department of Chemistry, University of Oxford

Availability:

Open Access MS

A TOF mass spectrometer with an HP1100 chromatography system.
Waters MALDI Micro MX

Managed by:

Department of Chemistry, University of Oxford

Availability:

Trained user availability variable.

A small MALDI TOF system whihc runs both Linear (400-1000 Da) and Reflectron mode (above 10,00 Da). It's used most extensively for peptide and small ...
Waters Quattro Micro

Managed by:

Department of Chemistry, University of Oxford

Availability:

Trained user availability variable.

A benchtop triple quadrupole instrument with a electrospray source and a quadrupole analyser. It's used primarily as an LC/MS system for the biological MS and ...
Waters Synapt HDMS

Managed by:

Department of Chemistry, University of Oxford

Availability:

MS services 24 hour turnaround; trained user availability variable.

A high resolution QTOF instrument with an ion-mobility cell. Instrument has a modified 8 Kd quadrupole and is currently used mainly for proteomic applications. With ...
Waters Xevo GS-2

Managed by:

Department of Chemistry, University of Oxford

Availability:

Heavily used.

High resolution QTOF system coupled to both a Waters Acquity UPLC
Waters Xevo GS-2-S

Managed by:

Department of Chemistry, University of Oxford

High resolution QTOF system coupled to both a Waters Acquity UPLC and Waters Acquity UPC².
XPS System

Managed by:

Department of Chemistry, University of Oxford

Availability:

http://saf.chem.ox.ac.uk/booking-oxford.aspx

Electrochemical Liquid Cell for non-volatile liquids.
XPS System

Managed by:

Department of Chemistry, University of Oxford

Availability:

http://saf.chem.ox.ac.uk/booking-oxford.aspx

Clam 4 hemispherical analyser.